Advanced Ceramic Processing and Technology by Binner J.G.P. ed. Noyes

By Binner J.G.P. ed. Noyes

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Values. RESULTS AND DISCUSSIONS f%wder Synthesis The synthesis process are listed conditions Figure are and Characterization conditions in Table presented 2: TEM micrograph 1. utilized to produce Si3N4 powders by the The properties in Table 2. Figure of as synthesized laser of powders produced under such 2 is a Si3N4 TEM micrograph powders. of the Bar = 100 nm. 6x1 O3 Han_2 Silane Atnmonia Argon: annulus chamber Reactor pressure Flame temperature Laser i ntensi ty Table 1: Si3N4 powder Surface Particle synthesis area size: He-pycncmetric Crystallinity Chemistry Table 2: Si3N4 powder conditions.

D. Kingery. Joint Publ. of the Technology Press of MIT and J. Wiley, NY. (1959). 16. Sintering of crystalline oxide, I. D. , Interaction between grain boundaries and pores. A. F. (Eds), 471-98, Gordon Breach (1967). 17. , On the effects of dihedral angle and pressure force for pore growth or shrinkage. Unpublished manuscript 18. Hoge. solid 19. Kellett. Sintering stability 20. Kellett, 5. J. and Lange, F. , Experimental relation between Ceram. Sot. (in review). 21. , 67 83 (1984). 22. Greskovich, C.

23). 24). than Si3N4 sintering boundary) other provided density thermodynamic extensive (or sinter theoretical of Silicon low of relative (32). However, 72 The fact a secondary that oxynitride to water phase in the attack may act et N2-204 vapor, vapor layer Miyamoto laser atmospheres on exposure Water This will Recent an amorphous of hours. formation. ;1)_ al. 1 compacts, of an through of form Si3N4 system oxide the layer, and application of for the the high acid powders. to In size, dispersed in density, study the particular, both exposed a non-aqueous uniformly packed with following th e high reasons: solvent (1) and oxygen green solutions density, the dispersant is dispersions (3) essential and for commonly and (5) was uniformly both contaminiation, activity have have the a Unamine low TM good dispersions, prepared Unamine by TM the should (32).

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